Français Русский Español Deutsch Bahasa Indonesia Tiếng Việt 한국어 ภาษาไทย हिन्दी العربية Português 日本語 English 中文
Determination of chlorine in polyphenylene sulfide2026-03-19  view:81

1.Test procedures

Weigh 0.05g of the sample, perform the test according to the set testing procedure, and observe the stability of the test results.

 

2.Combustion conditions

Temperature: 1100℃                 Oxygen: 0.4L/min             

Argon(carrier): 0.2L/min               Argon flow for humidification: 0.1L/min          

Water vapor: 0.1L/min                Absorption solution: pure water


Instrument:SDXNS200H

Combustion process

Step

Sample Introduction Time (s)

Distance (mm)

Retention Time (s)

Step 1

17

160

100

Step 1

100

30

100

Step 3

100

20

100

Step 4

30

100

100

 

3.IC conditions

Analytical Column: IonPac AS19 2*250mm   Guard Column: IonPac AG19 2*50mm

Eluent: EGC Ш KOH, 20mM, 0.25mL/min    Column temp.: 30℃

Quantitative loop: 400ul                                Linear range:1-10mg/L

Detector: Dionex-ADRS 600

 

4.Test results

 

 

Sample

Sample mass (g)

Conc. 

(mg/L)

Constant vol. (mL)

Measured Conc. (mg/kg)

polyphenylene sulfide

0.0521

6.72

20.46

2649

0.0517

6.69

2648

0.0498

6.43

2642

0.0479

6.21

2653

0.0511

6.62

2651

0.0499

6.46

2649

Aver.

2649

RSD(%)

0.14

Sales Contact
tel 0086 731 88112150
fax 0086 731 88134650
email sales@sandegroup.com
Service Contact
tel 0086 731 89864000
fax 0086 731 88134650
email service@sandegroup.com
Copyright©HunanSundy Science and Technology Co., Ltd.
湘ICP备10204722号