1.Test procedures
Weigh 0.05g of the sample, perform the test according to the set testing procedure, and observe the stability of the test results.
2.Combustion conditions
Temperature: 1100℃ Oxygen: 0.4L/min
Argon(carrier): 0.2L/min Argon flow for humidification: 0.1L/min
Water vapor: 0.1L/min Absorption solution: pure water
Combustion process
Step | Sample Introduction Time (s) | Distance (mm) | Retention Time (s) |
Step 1 | 17 | 160 | 100 |
Step 1 | 100 | 30 | 100 |
Step 3 | 100 | 20 | 100 |
Step 4 | 30 | 100 | 100 |
3.IC conditions
Analytical Column: IonPac AS19 2*250mm Guard Column: IonPac AG19 2*50mm
Eluent: EGC Ш KOH, 20mM, 0.25mL/min Column temp.: 30℃
Quantitative loop: 400ul Linear range:1-10mg/L
Detector: Dionex-ADRS 600
4.Test results

Sample | Sample mass (g) | Conc. (mg/L) | Constant vol. (mL) | Measured Conc. (mg/kg) |
polyphenylene sulfide | 0.0521 | 6.72 | 20.46 | 2649 |
0.0517 | 6.69 | 2648 | ||
0.0498 | 6.43 | 2642 | ||
0.0479 | 6.21 | 2653 | ||
0.0511 | 6.62 | 2651 | ||
0.0499 | 6.46 | 2649 | ||
Aver. | 2649 | |||
RSD(%) | 0.14 | |||